Experiment 497987

Compounds isolated

Details

PropertyValue
Pharmacology
Administration routeIN RATION
OrganismEmpty organism
CitationALONSO-AMELOT,M: CASTILLO,U: DE JONGH,F:. (1993). PASSAGE OF THE BRACKEN FERN CARCINOGEN PTAQUILOSIDE INTO BOVINE MILK.. 73(3)
Amount utilized
Compound isolated
DiseasePTAQUILOSIDE HAS BEEN DISCOVERED FOR THE FIRST TIME IN MILK SAMPLES OF A BOVINE FED A DIETARY COMPLEMENT (6 KG FRESH WEIGHT/DAY) OF FRESHLY CUT BRACKEN FRONDS. THIS WAS EQUIVALENT TO CA 216 MG/DAY PURE PTAQUILOSIDE. THE COMPOUND WAS FOUND IN A QUANTITY OF NO LESS THAN 0.11 MG/L IN MILK. THIS WAS DETERMINED BY THE APPEARANCE OF PTEROSIN B - THE DECOMPOSITION PRODUCT OF PTAQUILOSIDE - IN PREPURIFIED MILK SAMPLES TREATED WITH MILD ALKALI (PH 8.0 AND 11.5). THE LACK OF BASE TREATMENT LED TO THE ABSENCE OF PTEROSIN B. A MILK PREPURIFICATION PROTOCOL BASED ON METHANOL-ACETONITRILE PRECIPITATIONS IN SUCCESSION, HEXANE AND DICHLOROMETHANE EXTRACTIONS, ALKALINE TREATMENT, REEXTRACTION AND SILICA GEL MICROCOLUMN CHROMATOGRAPHY FOLLOWED BY REVERSE-PHASE HPLC WAS DEVELOPED FOR THE DETECTION OF PTAQUILOSIDE.
Number1
Qualitative resultACTIVE
AnimalCOW
Dose expressionDOSE